Paper
Determination of total cyanide in soil by isotope dilution GC/MS following pentafluorobenzyl derivatization.
Published Apr 8, 2017 · B. Campanella, L. Biancalana, Lucia D'ulivo
Analytica chimica acta
Q1 SJR score
15
Citations
0
Influential Citations
Abstract
Abstract hidden due to publisher request; this does not indicate any issues with the research. Click the full text link above to read the abstract and view the original source.
Study Snapshot
This novel method for determining total cyanide in soil samples based on single-step derivatization with pentafluorobenzyl bromide and isotope dilution GC/MS provides a sensitive and valid method for assessing soil cyanide levels.
PopulationOlder adults (50-71 years)
Sample size24
MethodsObservational
OutcomesBody Mass Index projections
ResultsSocial networks mitigate obesity in older groups.
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References
Pentafluorobenzyl bromide-A versatile derivatization agent in chromatography and mass spectrometry: I. Analysis of inorganic anions and organophosphates.
PFB-Br is a versatile derivatization agent for sensitive analysis of inorganic anions and organophosphates in biological samples, particularly plasma, urine, and saliva.
2017·33citations·D. Tsikas·Journal of chromatography. B, Analytical technologies in the biomedical and life sciences
Journal of chromatography. B, Analytical technologies in the biomedical and life sciences
Blank Correction in Isotope Dilution.
Blank-matching isotope dilution eliminates procedural blank bias and allows for direct determination of results without further corrections, making it a primary method for analysis without bias.
2015·7citations·E. Pagliano et al.·Analytical chemistry
Analytical chemistry
Calibration graphs in isotope dilution mass spectrometry.
The Padé approximant can accurately determine the curvature of isotope dilution curves, eliminating potential errors in chemical measurements.
2015·30citations·E. Pagliano et al.·Analytica chimica acta
Analytica chimica acta
The fate of cyanide in leach wastes at gold mines: An environmental perspective
Cyanide in gold mine wastes can pose a risk to aquatic organisms, and designing mineral processing operations with offgassing, aeration, and sunlight exposure can maximize environmental safety.
2015·138citations·C. Johnson·Applied Geochemistry
Applied Geochemistry
Derivatization method of free cyanide including cyanogen chloride for the sensitive analysis of cyanide in chlorinated drinking water by liquid chromatography-tandem mass spectrometry.
The developed derivatization method effectively detects and quantifies cyanide in chlorinated drinking water, with a detection limit of 0.07 g/L and interday relative standard deviation less than 4%.
2015·35citations·Hye-In Kang et al.·Analytical chemistry
Analytical chemistry
Citations
Method for Screening Sodium Cyanoborohydride for Free Cyanide Content and Its Impact on Bioconjugation Chemistry.
This study presents a simple chromatographic assay for quantifying free cyanide in sodium cyanoborohydride, which can help minimize undesired side products and improve bioconjugation chemistry in the pharmaceutical industry.
2025·0citations·Jarrod P Cohen et al.·Bioconjugate chemistry
Bioconjugate chemistry
Simultaneous determination of cyanide and thiocyanate in milk by GC-MS/MS using cetyltrimethylammonium bromide as both phase transfer catalyst and protein precipitant
The developed method for simultaneous determination of cyanide and thiocyanate in milk by GC-MS/MS using cetyltrimethylammonium bromide is a simple, fast, and highly sensitive method.
2023·0citations·Xing Li et al.·Food Additives & Contaminants: Part A
Food Additives & Contaminants: Part A
Synthesis of gold nanoclusters-loaded lysozyme nanoparticles for ratiometric fluorescent detection of cyanide in tap water, cyanogenic glycoside-containing plants, and soils.
LysNP-AuNCs, a dual-emission probe, effectively detect cyanide in tap water, soils, and cyanogenic glycoside-containing plants without additional fluorophores.
2021·18citations·Wei‐Bin Tseng et al.·Environmental research
Environmental research
Determination of Cyanide in Blood for Forensic Toxicology Purposes—A Novel Nci Gc-Ms/Ms Technique
The novel GC-MS technique using a triple quadrupole mass spectrometer enhances selectivity and sensitivity for cyanide determination in blood, making it suitable for forensic toxicology studies.
2021·6citations·Marcin Osak et al.·Molecules
Molecules
The detoxification and utilization of cyanide tailings: A critical review
Thermal treatment with catalysts and autoclaved hydrolysis show promising technologies for detoxifying cyanide tailings, removing cyanides over 99%, potentially bringing economic and environmental benefits.
2021·67citations·Kai-wei Dong et al.·Journal of Cleaner Production
Journal of Cleaner Production
Efficient destruction of sodium cyanide by thermal decomposition with addition of ferric oxide
Ferric oxide addition significantly accelerates the thermal decomposition of sodium cyanide, enabling its complete destruction within 30 minutes in air or O2.
2021·6citations·Kai-wei Dong et al.·Transactions of Nonferrous Metals Society of China
Transactions of Nonferrous Metals Society of China
Gas chromatography-mass spectrometric identification of cyanide using a nucleophilic substitution based derivatization with S-phenyl benzenethiosulfonate.
The developed method for GC-MS based cyanide identification using S-phenyl benzenethiosulfonate provides a simple, efficient, and accurate method for analyzing aqueous samples containing cyanide salts.
2020·3citations·D. R. Goud et al.·Analytical methods : advancing methods and applications
Analytical methods : advancing methods and applications