Paper
Electro-oxidation of catechols in the presence of benzenesulfinic acid. Application to electro-organic synthesis of new sulfone derivatives
Published Feb 22, 2002 · D. Nematollahi, R. Rahchamani
Journal of Electroanalytical Chemistry
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60
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0
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Abstract
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Study Snapshot
Electrochemical oxidation of catechols in the presence of benzenesulfinic acid leads to the successful synthesis of new sulfone derivatives in good yields and purity.
PopulationOlder adults (50-71 years)
Sample size24
MethodsObservational
OutcomesBody Mass Index projections
ResultsSocial networks mitigate obesity in older groups.
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References
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Electrochemical oxidation of catechol and 4-methylcatechol in methanol leads to the successful synthesis of 4,5-dimethoxy- and 4-methoxy-5-methyl-o-benzoquinone with 95% and 85% yields respectively.
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Substituted catechols undergo electrochemical oxidation to produce unstable dimeric products, often polymerizing or undergoing irreversible reactions.
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The novel DDPHC diazonium salt (DDPHC-DAS) effectively determines phenol and chlorophenol derivatives using CV, SWV, and DPV techniques, providing a cost-effective method for these compounds.
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