Paper
Ethyl 1‐Naphthylacetate
Published Apr 28, 2003 · V. Lee, M. Newman
Organic Syntheses
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Abstract
Ethyl 1-Naphthylacetate reactant: 30.5 g. (0.160 mole) of 1-naphthoyl chloride intermediate: 1-(diazoacetyl)naphthalene product: ethyl 1-naphthylacetate reactant: 1-naphthoic acid reactant: 1-bromonaphthalene solvent: propyl 1-naphthylacetate Keywords: diazotization, preparation of diazonium salts; esterification, of substituted monobasic acids; rearrangements; assay methods, for diazomethane; diethyl ether; 1-naphthoyl chloride, preparation of; silver benzoate, preparation of; 1-(diazoacetyl)naphthalene, skin irritant; diazomethane, explosive, toxic
Ethyl 1-naphthylacetate is prepared by diazotization, esterification, and rearrangements, with 1-(diazoacetyl)naphthalene being a skin irritant and diazomethane being an explosive and toxic compound.
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