Reduction of 3,5-dinitro-2-pyridyl derivatives with sodium borohydride part II. Application of proton nuclear magnetic resonance spectroscopy to structure problems

doi:10.1039/J29700001567

Paper

Reduction of 3,5-dinitro-2-pyridyl derivatives with sodium borohydride part II. Application of proton nuclear magnetic resonance spectroscopy to structure problems

Published 1970 · E. Bordignon, A. Signor, I. Fletcher

Journal of The Chemical Society B: Physical Organic

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Abstract

The mechanism of the reduction of 2-methylamino-3,5-dinitropyridine is elucidated by carrying out the reaction with sodium boro-hydride and -deuteride in water and deuterium oxide as solvents. The tautomeric structure and stereochemistry of the tetrahydro-reduction product is discussed with reference to the n.m.r. spectra.

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The mechanism of reduction of 2-methylamino-3,5-dinitropyridine with sodium borohydride and -deuteride in water and deuterium oxide reveals the tautomeric structure and stereochemistry of the tetrahydro-reduction product.

PopulationOlder adults (50-71 years)

Sample size24

MethodsObservational

OutcomesBody Mass Index projections

ResultsSocial networks mitigate obesity in older groups.

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Reduction of 3,5-dinitro-2-pyridyl derivatives with sodium borohydride part II. Application of proton nuclear magnetic resonance spectroscopy to structure problems

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