Study on synthesis of 3-chloro-4-[1,1,2-trifluoro-2-(trifluoromethoxy)-ethoxy] aniline

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Study on synthesis of 3-chloro-4-[1,1,2-trifluoro-2-(trifluoromethoxy)-ethoxy] aniline

Published 2007 · Wen Zi-qiang

Applied Chemical Industry

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Abstract

2-Chloro-4-aminophenol was synthesized from 3,4-dichloronitrobenzene by high pressure hydrolysis and reduction reaction,afterwards the addition reaction with perfluoro-vinyl-perfluoro-methyl ether was conducted to synthesize 3-chloro-4-[1,1,2-trifluoro-2-(trifluoromethoxy)-ethoxy]aniline.The overall yield was 72.0%,the product structure was characterized by elemental analyses,IR spectra and 1H NMR,it has characteristics of ready availability of reactant,high yield,good quality,little pollution to environment.

Study Snapshot

This study successfully synthesized 3-chloro-4-[1,1,2-trifluoro-2-(trifluoromethoxy)-ethoxy] aniline from 2,4-dichloronitrobenzene with high yield, good quality, and minimal environmental pollution.

PopulationOlder adults (50-71 years)

Sample size24

MethodsObservational

OutcomesBody Mass Index projections

ResultsSocial networks mitigate obesity in older groups.

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Study on synthesis of 3-chloro-4-[1,1,2-trifluoro-2-(trifluoromethoxy)-ethoxy] aniline

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