Study on the Synthetic Technology of(R)-3-aminotetrahydrofuran

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Study on the Synthetic Technology of(R)-3-aminotetrahydrofuran

Published 2012 · Yang Jianping

Guangzhou Chemical Industry

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Abstract

The(R)-3-aminotetrahydrofuran was synthesized using(S)-3-hydroxyltetrahydrofuran by acylation with 4-methylbenzensulfonyl Chloride,substitution with NaN3 and reduction with Zn/NH4Cl.The result showed that it obtained the higher yield of amine reducted the organic azide with the Zn/NH4Cl.All compounds were confirmed by the methods of IR,HNMR and MS.This method was more economical compared with the reported methods.

Study Snapshot

This study presents a more economical method for synthesizing (R)-3-aminotetrahydrofuran using (S)-3-hydroxyltetrahydrofuran, 4-methylbenzensulfonyl chloride, NaN3 and reduction with Zn/NH4Cl, resulting

PopulationOlder adults (50-71 years)

Sample size24

MethodsObservational

OutcomesBody Mass Index projections

ResultsSocial networks mitigate obesity in older groups.

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Study on the Synthetic Technology of(R)-3-aminotetrahydrofuran

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