Paper
The Synthesis of 4-Chloropiperidine Hydrochloride
Published 2010 ยท Zhang Guan-you
Shandong Chemical Industry
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Abstract
Used piperidin-4-one hydrochloride as raw materials,through the reduction and n-carbonylation of tert-butyloxyl to obtain the tert-butyl-4-hydroxy pi-peridine-l-carboxylate.The yield was 65%.Then synthesized 4-chloropiperidine hydrochloride with sulfoxyl chloride.The yield was 50.9%.
Study Snapshot
4-Chloropiperidine hydrochloride can be synthesized with sulfoxyl chloride, achieving a yield of 50.9%.
PopulationOlder adults (50-71 years)
Sample size24
MethodsObservational
OutcomesBody Mass Index projections
ResultsSocial networks mitigate obesity in older groups.
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