Synthesis and characterization of 2,2-dimethylolheptanoic acid

Paper

Synthesis and characterization of 2,2-dimethylolheptanoic acid

Published 2011 · W. Yun

Applied Chemical Industry

UNKNOWN SJR score

0

Citations

0

Influential Citations

Semantic Scholar

Abstract

2,2-Dimethylolheptanoic acid was prepared from 2,2-dimethylolheptaldehyde and hydrogen peroxide via oxidation.The structure of 2,2-dimethylolheptanoic acid was confirmed by IR and 1H NMR and 13C NMR.The results showed that the optimun conditions were as follows:molar ratio of hydrogen peroxide to 2,2-dimethylolheptaldehyde was 1.1∶1,reaction time was 8 h,the quality ratio of water to 2,2-dimethylolheptaldehyde was 3∶1,reaction temperature was 70 ℃,pH value was 4.The yield of 2,2-dimethylolheptanoic acid was 57.6%.

Study Snapshot

The optimal conditions for preparing 2,2-dimethylolheptanoic acid are 1.1:1 hydrogen peroxide:2,2-dimethylolheptaldehyde ratio, 8 hours reaction time, 3:1 water:2,2-dimethylolheptaldehyde ratio

PopulationOlder adults (50-71 years)

Sample size24

MethodsObservational

OutcomesBody Mass Index projections

ResultsSocial networks mitigate obesity in older groups.

Sign up to use Study Snapshot

Consensus is limited without an account. Create an account or sign in to get more searches and use the Study Snapshot.

Create an account

Synthesis and characterization of 2,2-dimethylolheptanoic acid

Sign up to use Study Snapshot

References

Citations