Synthesis and Crystal Structure of (4S)-5-(2-Methoxy-2-oxoethylamino)-5-oxo- 4-(3,4,5-trimethoxybenzamido) Pentanoic Acid

Paper

Synthesis and Crystal Structure of (4S)-5-(2-Methoxy-2-oxoethylamino)-5-oxo- 4-(3,4,5-trimethoxybenzamido) Pentanoic Acid

Published 2005 · X. Wen

Chinese Journal of Structural Chemistry

UNKNOWN SJR score

0

Citations

0

Influential Citations

Semantic Scholar

Abstract

The crystal structure of (4S)-5-(2-methoxy-2-oxoethylamino)-5-oxo-4-(3,4,5- trimethoxybenzamido) pentanoic acid 5 (C18H24N2O9, Mr = 412.39) has been determined by single- crystal X-ray diffraction analysis. The crystal belongs to monoclinic, space group P21/c with a = 27.665(9), b = 5.1444(16), c = 13.907(4) ?, β = 98.401(5)o, V = 1958.0(11) ?3, Z = 4, Dc = 1.399 g/cm3, μ = 0.113 mm-1, F(000) = 872, R = 0.0606 and wR = 0.1405 (I 2σ(I)). The results con- firmed that 5 could be assigned to the tautomeric form. The intermolecular hydrogen bonds between O(5)–H(5)…O(7), N(2)–H(2)…O(6) and N(1)–H(1)…O(4) have been observed.

Study Snapshot

The crystal structure of (4S)-5-(2-methoxy-2-oxoethylamino)-5-oxo-4-(3,4,5-trimethoxybenzamido) pentanoic acid confirms its tautomeric form and shows intermolecular hydrogen bonds between O

PopulationOlder adults (50-71 years)

Sample size24

MethodsObservational

OutcomesBody Mass Index projections

ResultsSocial networks mitigate obesity in older groups.

Sign up to use Study Snapshot

Consensus is limited without an account. Create an account or sign in to get more searches and use the Study Snapshot.

Create an account

Synthesis and Crystal Structure of (4S)-5-(2-Methoxy-2-oxoethylamino)-5-oxo- 4-(3,4,5-trimethoxybenzamido) Pentanoic Acid

Sign up to use Study Snapshot

References

Citations