Ethyl 2-ethoxycarbonyl-3,5-dioxoiiexanoate (1-b) was synthesized by the hydrogenolysis and hydrolysis of diethyl (3-methyl-5-isoxazolyl)malonate (3-b), which was obtained by the di-carboxylation of 3,5-dimethylisoxazole (4) with ethyl cyanoformate in the presence of butyllithium.

This study demonstrates the potential of this method for the synthesis of ethyl 2-ethoxycarbonyl-3,5-dioxoiiexanoate, a promising intermediate in the synthesis of ethyl 2-ethoxycarbonyl-3,5-dio

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THE SYNTHESIS OF ETHYL 2-ETHOXYCARBONYL-3,5-DIOXOHEXANOATE

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