Synthesis,Crystal-structure and Thermal Properties of (5-Fluoro-2,4-dioxo-3,4-dihydropyrimidin-1(2H)-yl) Methyl Thiophene-2-carboxylate

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Synthesis,Crystal-structure and Thermal Properties of (5-Fluoro-2,4-dioxo-3,4-dihydropyrimidin-1(2H)-yl) Methyl Thiophene-2-carboxylate

Published 2009 · Hu Miaolin

Journal of Wenzhou University

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Abstract

A new 5-fluorouracil derivative,(5-fluoro-2,4-dioxo-3,4-dihydropyrimidin-1(2H)-yl) methyl thiophene-2-carboxylate,has been synthesized.Its structure has been characterized by means of 1H NMR,13C NMR,IR.Single crystal was diffracted with X-ray to ascertain the crystal structure of the compound.And the thermal feature of the compound was analyzed.Crystal data are shown as following:monoclinic,space group P2/c,a=9.613 4(14),b=4.838 1(7),c=24.534(4),α=90°,β=97.289(3)°,γ=90°,Z=4,F(000)=552,R1= 0.061 6.

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The crystal structure and thermal properties of (5-fluoro-2,4-dioxo-3,4-dihydropyrimidin-1(2H)-yl) methyl thiophene-2-carboxylate show that it is a monoclinic compound with a P2/c

PopulationOlder adults (50-71 years)

Sample size24

MethodsObservational

OutcomesBody Mass Index projections

ResultsSocial networks mitigate obesity in older groups.

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Synthesis,Crystal-structure and Thermal Properties of (5-Fluoro-2,4-dioxo-3,4-dihydropyrimidin-1(2H)-yl) Methyl Thiophene-2-carboxylate

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