H. Derks, H. Wynberg
Nov 1, 1983
Citations
0
Influential Citations
3
Citations
Journal
Journal of Labelled Compounds and Radiopharmaceuticals
Abstract
[1,1,1,6,6,6-d6]-E-3,4-di-(4-hydroxyphenyl)-hex-3-ene was synthesized from [1,1,1-d3]-4-methoxypropiophenone by reductive coupling. The preparation of [1,1,1-d3]-4-methoxypropiophenone involved reaction of p-anisoylchloride with perdeuterated diethyl-cadmium followed by back-exchange of the alpha protons.