I. Grapsas, S. Mobashery
Apr 15, 2001
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Abstract
[41864-24-8] C7H11N3O2 (MW 169.18) InChI = 1S/C7H11N3O2/c1-7(2,3)12-6(11)10-5-8-4-9-10/h4-5H,1-3H3 InChIKey = XWUFRDJEUOAMNW-UHFFFAOYSA-N (a reagent for protection of amines with the tert-butoxycarbonyl group1) Physical Data: mp 40 °C. Solubility: sol DMF and DMSO. Form Supplied in: the reagent is commercially available and is supplied as a solid. Preparative Method: 1-tert-butoxycarbonyl-1,2,4-triazole 1 is available commercially, but it can readily be prepared from the reaction of tert-butoxycarbonyl azide with 1-trimethylsilyl-1,2,4-triazole or reaction of tert-butanol with N,N′-carbonyl-di-1,2,4-triazole in high yield.1 Handling, Storage, and Precautions: anhydrous conditions are recommended for reactions, and the reagent is best stored at 0–4 °C.