Deamination in ethyl acetate media

Paper

Deamination in ethyl acetate media

Published 2005 · Meng Xiao-yan, Cai Chun

Chemical Reagents

UNKNOWN SJR score

1

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0

Influential Citations

Semantic Scholar

Abstract

In ethyl acetate media 2,6-dichloro-4-nitroaniline reacted to give 3,5-dichloronitrobenzene through diazotization and reductive deamination in one-pot.Ethyl acetate displayed not only as a solvent for two-phase reaction,but also as a pro-reducing (agent).The process was satisfactory with little pollution of waste acid and waste gas and had no by-products(e.g.ether).The factors including amounts of sodium nitrite,sulfuric acid and ethyl acetate,and reaction temperature were investigated.

Study Snapshot

Ethyl acetate media effectively deaminates 2,6-dichloro-4-nitroaniline to 3,5-dichloronitrobenzene in one-pot, with minimal waste acid and gas pollution and no by-products.

PopulationOlder adults (50-71 years)

Sample size24

MethodsObservational

OutcomesBody Mass Index projections

ResultsSocial networks mitigate obesity in older groups.

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Paper

Deamination in ethyl acetate media

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References

Citations

Efficient synthesis of glutaric acid from l-glutamic acid via diazoniation/hydrogenation sequence

This study successfully synthesized glutaric acid from l-glutamic acid using a one-pot diazoniation/hydrogenation sequence, offering a practical approach for its production.