P. Dragovich, D. Murphy, Chinh Tran
May 23, 2008
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0
Influential Citations
4
Citations
Journal
Synthetic Communications
Abstract
Abstract A novel synthesis of 2-amino-5-methanesulfonylaminobenzenesulfonamide is described. This preparation begins with readily available 4-nitroaniline and proceeds through five steps (isolations) in 41% overall yield. The described chemistry is conducted on a 50- to 100-g scale and does not require extractive workup procedures or chromatographic purifications.