Han Jianrong
2013
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Journal
Journal of Hebei Normal University
Abstract
3-methoxyhexanoic acid was prepared from ethyl 3-hydroxy-hexanoate by nucleophilic substitution reaction using iodomethane,dimethyl sulfate,and diazomethane as methylation reagent.The influences of different reaction conditions on the yield,such as solvents and the catalysts,were discussed.The optimal reaction conditions of 3-methoxyhexanoic acid were explored.The structure of the 3-methoxyhexanoic acid was characteried by 1HNMR and elemental analysis.