Li Che
2014
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Journal
Guangzhou Chemical Industry
Abstract
Acetylacetonatodicarbonylrhodium(Ⅰ) as an important oxo industrial catalyst precursor was prepared from trisodium hexachlororhodate as rhodium material,with the yield of 96% after the optimized reaction conditions.The structure of the compound was characterized by IR,H-NMR and C-NMR.This process can simplify the preparation steps of acetylacetonatodicarbonylrhodium(Ⅰ) from rhodium powder to shorten the production cycle and reduce production costs.