Zhang Bin
2008
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Journal
Chemical Reagents
Abstract
Tri(m-ethoxyphenyl)bismuthine was synthesized by mixing the Grignard reagent with trichlorobismuthine.The structure of the target compound was characterized by elemental analysis and IR spectroscopy.The crystal structure was determined by the X-ray diffraction method.Its crystals belonged to the orthorhombic system with a space group of P212121 and the following cell parameters:a=0.631 4(2) nm,b=1.501 1(4) nm,c=2.380 8(6) nm,V=2.256 6(9) nm3,Dc=1.685 g/cm3,μ=7.833 mm-1,F(000)=1 112,Z=4,R1=0.045 7,and wR2=0.096 2.