Zhu Xun
2012
Citations
0
Influential Citations
0
Citations
Journal
Chemical Reagents
Abstract
5-(Benzylmercapto)-1H-tetrazole was synthesized with the hexadecyl trimethyl ammonium bromide as phase transfer catalyst and water/ethanol as solvent.The optimum conditions were obtained as follows:molar ratio is 1∶1.2∶1.2,the reaction temperature is 95 ℃(refluxing temperature),and the reaction time is 16 h.The yield is 85.2%.The process is conenient operation with high yield and low pollution and it is suitable for industrial production,and has wide prospect of application.