Chen Rong-gu
2015
Citations
0
Influential Citations
0
Citations
Journal
Journal of Fujian Normal University
Abstract
6-[N,N-bis( 2-hydroxyethyl) amine]-2,4-dichloro-1,3,5-triazine( referred to as1) was synthesized from cyanuric chloride( CYC) and diethanolamine( DEA) in mixed medium of acetone and water.The structure of 1 was characterized by element analysis,FTIR,1H NMR and13 C NMR.The reaction conditions,such as reaction media,base catalysts,the mol ratio of raw materials and reaction time,were investigated.It was found that the optimal reaction conditions for synthesis of1 was as follows: CYC was 0.01 mol,n( CYC) ∶ n( DEA) was 1 ∶ 1,reacting at 0 ~ 5 ℃ for 2 h in the mixed medium of V( acetone) ∶ V( water) = 1 ∶ 1.