J. Heng
2006
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Journal
Chemical Research
Abstract
Aluminium acetylacetonate was prepared by grinding inorganic aluminum salts and acetylacetone(Hacac) at room temperature.Solid bases were used to promote the reaction.The kinds and amount of solid base,the mole ratio of reactants,and grinding time were investigated.The yield of the solid state grinding method is higher(more than 90%)compared with the traditional method.The product was confirmed by FTIR and TG analyses.The optimum reaction condition is as follows: mole ratio of Al~(3+) to Hacac is 10 / 40,solid bases as required,grinding for 1 h at room temperature.