Jiang Du-xiao
2005
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Journal
Chinese Journal of Synthetic Chemistry
Abstract
3-Amino-4-aminomethylbenzenesulfonate was synthesized from o-nitrotoluene by sulphonation,photochloration,Holfmann amination and hydrazine hydrate reduction.The structure was identified by ~1H NMR,IR,MS and elemental analysis.The purity and yield reached to 99.2%(HPLC) and 62.8%,respectively.