T. Zhu
2011
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Journal
Journal of Guizhou University
Abstract
A compound 3,9-di(1H-pyrrol-2-yl)-2,4,8,10-tetraazaspiro[5.5]undecane was synthesized and structurally characterized by single crystal X-ray diffraction structural determination.Crystal data: a=8.386(2),b=10.541(3),c=0.779(3),α=87.274(10)°,β= 87.769(10)°,γ=84.38 7(10)°,V=946.6(4)3.The compound is constitute of 3,9-di(1H-pyrrol-2-yl)-2,4,8,10-tetraaz-aspiro[5.5]undecane and four water molecules,The water molecules and the N atoms from the pyrrol rings of 3,9-di(1H-pyrrol-2-yl)-2,4,8,10-tetraazaspiro[5.5]undecane are linked into one-dimensional supramolecular chain,and the chain structure further forms two-dimensional supramolecular network structure by intermolecular hydrogen bonds.