Wang Qian-y
2015
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Journal
Fine Chemical Intermediates
Abstract
N-Boc-1,2,3,5-tetrahydro spiro [ benzo [ c] azepine-4,2-piperidine] was synthetized using1-Boc-piperidine-2-carboxylic acid metyl ester and 2-bromomethyl- benzonitrile as the raw materials followed by nucleophilic substitution reaction, cyano-reduction reaction, and cyclization reaction. The chemical structure of this novel compound was characterized using1 H NMR,13 C NMR and High Resolution Mass Spectrometry, and a yield of 48% was obtained.