Chen Zheng-guo
2011
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Journal
Fine Chemical Intermediates
Abstract
Sodium 3-chloro-2-hydroxy propanephosphate was synthesized from epichlorohydrin and sodium dihydrogen phosphate.The affecting factors including different kinds of phosphate,the molar ratio of reactants,the reaction temperature,time and pH value were investigated and optimized.The product was obtained in 77.9% yield and its structure was verified by IR and 1H NMR.