N. Xu, Yan Ouyang, D. Liao
Aug 10, 2006
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Influential Citations
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Journal
Journal of Chemical Crystallography
Abstract
A novel tetrachlorophthalato-Yb(III) complex [Yb(tcph)(H2O)7]Htcph·H2tcph·H2O (1) (H2tcph=tetrachlorophthalic acid) has been synthesized and characterized by the single crystal X-ray diffraction analysis. Colorless crystals of 1 crystallize in the triclinic space group P-1, with a=6.8504(5) Å, b=16.1921(12) Å, c=19.0123(14) Å and α=67.4470(10)°, β=86.5290(10)°, γ=81.6480(10)°, V=2.113 g/cm3 and Z=2. Unique reflections with I > 2σ(I) on refinement afford values of R1=0.0219 and wR2=0.0565.