Ying Shii-liang
2005
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Journal
Journal of Nanchang University
Abstract
Methyldiethoxysilane was synthesized with CH_3SiHCl_2 and CH_3CH_2OH by alcoholysis methods (solution,acid acceptor,gas-liquid phase).The results showed that:solution method was the best,the MeSiH(OEt)_2 content of product was 78%.And the perfect conditions of synthesizing methyldiethoxysilane were:n-hexane used as solution,the molar ratio CH_3SiHCl_2 and CH_3CH_2OH being 1∶1.9,a certain speed of adding ethanol,reactive temperature 33 ℃,reactive time about 2 h.