W. Porter, L. A. Spitznagle, W. Trager
Oct 1, 1976
Citations
0
Influential Citations
6
Citations
Journal
Journal of Labelled Compounds and Radiopharmaceuticals
Abstract
Labeled silver carbonate was prepared from barium carbonate-13C or -14C and aqueous silver nitrate in 95 to 100% yield. Diethyl carbonate-13C or -14C was generated in 60 to 85% overall yield by treatment of labeled silver carbonate with ethyl iodide and tetraethylammonium iodide in dimethylformamide. The effects of alterations in reaction time, metal ion, solvent and catalyst were investigated.