R. Finke, T. N. Sorrell
Apr 28, 2003
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Journal
Organic Syntheses
Abstract
Nucleophilic Acylation with Disodium Tetracarbonylferrate: Methyl 7-Oxoheptanoate and Methyl 7-Oxooctanoate intermediate: Disodium tetracarbonylferrate sesquidioxanate product: Methyl 7-oxoheptanoate product: Methyl 7-oxooctanoate reactant: Methyl 6-bromohexanoate Keywords: acylation; esterification, of substituted monobasic acids; reduction, miscellaneous; dioxane; disodium tetracarbonylferrate sesquidioxanate; hexane; methyl 6-bromohexanoate, preparation of; N-methylpyrrolidinone; nitrogen, oxygen-free, preparation of; tetrahydrofuran; carbon monoxide; iron pentacarbonyl; methyl iodide; apparatus, for removal of supernatant solvent under inert atmosphere