R. Moriarty
May 16, 1991
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Abstract
Abstract : A series of monoazido alkanes and diazido alkanes have been synthesized. Specifically,1-azidobutane (100.0 g), 1-azidohexane (100.0 g), 1- azidooctane (100.0 g), and 1-azidoheptane (100.0 g), 1,3-diazidopropane (200.0 g), 1,4-diazidobutane (200.0 g, 1,5-diazidopentane (200.0 g), 1,6-diazidohexane (200.0 g), 1,7-diazidoheptane (200.0 g), 1,8-diazidooctane (200.0 g) were synthesized and characterized completely both analytically and spectroscopically. Among cyclic examples 1,2-diazidocyclopentane, 1,2- diazidocyclopentane, 1,2-diazidocyclohexane and 1,4-diazocyclohexane were synthesized. Norbornene was converted into a regioisomeric mixture of 2,3- diazido and syn and anti-2,7- diazidonorbornanes. The photodimer of nonbornadiene was synthesized and converted to the tetraazido analog.