P. Wipf, Wenjing Xu
Apr 28, 2003
Citations
0
Influential Citations
14
Citations
Journal
Organic Syntheses
Abstract
Allylic alcohols by alkene transfer from zirconium to zinc: 1-[(tert-butyldiphenylsilyl)oxy]-dec-3-en-5-ol intermediate: tert-butyl(but-3-ynyloxy)diphenylsilane product: 1-[(tert-butyldiphenyl-silyl)oxy]-dec-3-en-5-ol Keywords: alkenylation, C-alkenylation; Grignard and related reactions; protection, oxygen; dichloromethane (methylene chloride); chlorobis(η5-cyclopentadienyl)hydridozirconium = Schwartz's reagent; 4-dimethylaminopyridine, poison; flasks, equipped with gas inlet stopcock