B. Haveaux, A. Dekoker, M. Rens
Apr 28, 2003
Citations
0
Influential Citations
11
Citations
Journal
Organic Syntheses
Abstract
α-Chloro Enamines, Reactive Intermediates for Synthesis: 1-Chloro-N,N,2-Trimethylpropenylamine reactant: 115 g. (1.00 mole) of freshly distilled N,N-dimethylisobutyramide solvent: 150 ml. of dry, low-boiling petroleum ether product: 1-chloro-N,N,2-trimethylpropenylamine Keywords: elimination, dehydrohalogenation; enamine or imine formation; dichloromethane (methylene chloride); N,N-dimethylisobutyramide, preparation of; triethylamine; phosgene; apparatus, for chlorination, with phosgene