D. W. Phelps, A. W. Cordes
Jun 1, 1976
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0
Influential Citations
7
Citations
Journal
Journal of Heterocyclic Chemistry
Abstract
The structure of 2-(trifluoromethyl)phenothiazine, C13H8NSF3, was determined by single crystal X-ray diffraction. The molecule crystallizes in space group P212121, with a = 7.766(2), b = 5.957(1), and c = 23.499(5)A. The final R value is 0.073. The CSC bond angle is 102.0°, the CNC bond angle is 124.8°, and the dihedral angle between the phenylene planes is 171.2(1)°. The hydrogen atom bonded to the nitrogen atom was located; it is on the inside of the butterfly angle and the S…NH bond angle is 173.3°.