Heng-Shan Dong, B. Quan, Hui-Qian Tian
Nov 6, 2002
Citations
0
Influential Citations
4
Citations
Journal
Journal of Molecular Structure
Abstract
Abstract 3H-2-imino-4-methylbenzothiazoline was obtained from o-methylaniline to form 4. The yielded product 6 was confirmed by Elemental analyses, NMR, MS, IR spectra and X-ray crystallography. Compound 6, C8H8N2S, Mr=164.23, crystallized in the monoclinic space group P21/c with unit cell parameters a=4.0949(15), b=11.790(2), c=15.837(2) A , α=89.975(14), β=96.510(19), γ=90.09(2)°, V=759.7(3) A 3 , Z=4, D m =1.436 Mgm −3 . The intermolecular attraction of 3H-2-imino-4-methylbenzothiazoline in crystal structure is discussed.