Zhaole Lu
2014
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Journal
Journal of Changchun Normal University
Abstract
The outcome of the experiment is that benzyl triethyl chloride whose molecular structure is C13H22ClN,is a kind of effective phase transfer catalysts which can synthesise 4,4'-( phenylazanediyl) dibenzoic acid. During the synthesis process,4,4'-Dimethyltriphenylamine was used as raw material,in alkaline condition with Potassium Permanganate oxidation,and adding phase transfer catalyst to synthesis of 4,4'-( phenylazanediyl) dibenzoic acid. Research the reaction conditions were as follows: when the amount of Potassium permanganate is 7g,the Tert-butanol alcohol is 30ml,the amount of Benzyl triethyl chloride is 0. 50g,and the reflecting time is 5.5h,the product yield is up to 59. 4%.