Zhang Xiao-mei
2006
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Journal
Journal of Anhui University
Abstract
New bis-hydroxy compound bis-(3,5-dichloro-2-hydroxy oxyethyl phenyl) methane 3 was obtained by the reaction of LiAlH_(4) reducing compound 2 prepared by the reaction of bis-(3,5-dichloro-2-hydroxy phenyl) methane 1 with methyl chloro-acetate,and mono-hydroxylation product 4 was separated from the reacting mixture.The structures of 2,3 and 4 were characteristic by NMR,IR,MS and elemental analysis.The reasons causing low yield of 2 and 3 were discussed in the paper also.