G. Bandoli, A. Ongaro, A. Rubello
1998
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Journal
Crystal Research and Technology
Abstract
The structure of the title compound (C 9 H 13 NO 2 NaP.3H 2 O) (Toldimfos Na.3H 2 O) has been determined at room temperature. The crystals are monoclinic, a = 38.15(2) A, b = 4.940(3) A, c = 14.510(8) A, β = 109.58(4)°, V = 2576(3) A 3 , Z= 8, D calc = 1.419 g cm -3 , space group C2/c. The structure was solved by direct methods and refined by frill-matrix least-squares method (MoK α radiation; R = 0.061). Indexed powder diffraction pattern for the drug is also reported.