G. Zill, W. Ziegler, G. Engelhardt
1990
Citations
0
Influential Citations
22
Citations
Journal
Chemosphere
Abstract
Abstract Zearalenone-4-β- d -glucopyranoside was synthesized via a chemical reaction between zearalenone and 2,3,4,6-tetra-O-acetyl-α- d -glucopyranosylbromide, followed by deacetylation. By this way the exact molecular structure of the glucose conjugate, formerly isolated from corn tissue cultures was confirmed. For the simultaneous estimation of zearalenone, β-zearalenol and zearalenone-4-β- d -glucopyranoside a HPLC method was developed using fluorescence detection and a gradient solvent system.