B. Lakshminarayana, C. Gnanendra, T. N. M. Prasad
Feb 20, 2010
Citations
0
Influential Citations
5
Citations
Journal
Journal of Chemical Crystallography
Abstract
The novel 3-methyl-2,6-dip-toylpiperidine-4-one was acylated by 3-chloropropanoychloride and subjected for dehydrohalogenation. The synthesized compound was characterized by spectroscopic techniques and finally confirmed by X-ray diffraction studies. The molecule crystallizes in the monoclinic crystal class in the space group C2/c with cell parameters a = 18.538(2) Å, b = 9.9050(1) Å, c = 22.954(2) Å, β = 94.486(8)° and Z = 8. The piperidine ring adopts a twist boat conformation.Graphical AbstractThe title compound was synthesized by acylation of 3-methyl-2,6-dip-tolylpiperidin-4-one followed by dehydrohalogenation and recrystalisation in ethanol. The molecule crystallizes in the monoclinic crystal class in the space group C2/c with cell parameters a = 18.538(2)Å, b = 9.9050(1) Å, c = 22.954(2) Å, β = 94.486(8)° and Z = 8. The heterocyclic ring adopts a twisted boat conformation.