J. J. D'amico, C. Tung, W. E. Dahl
Jun 1, 1978
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Journal
ChemInform
Abstract
Abstract The reaction of potassium ethyl dithiocarbonate with 4-chloro-3,5-dinitrobenzotrifluoride in dimethylformamide at 25–30°C afforded the titled disulfide (1) and sulfide (2). Possible mechanism and supporting NMR, ir, Raman and mass spectral data are discussed. The assigned structure for 1 was verified by X-ray crystal structure analysis.