B. Lynn, E. Alley
1987
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0
Influential Citations
3
Citations
Journal
Journal of Chromatography A
Abstract
Abstract Derivatives of the cis and trans isomers of 1,2-, 1,3- and 1,4-diaminocyclohexanes were prepared by the reaction of the amine with benzaldehyde. These compounds were analyzed by gas chromatography on a DB-5, bonded phase, fused-silica capillary column resulting in a baseline separation for the six isomers providing accurate determination of the cis-to-trans ratios in a single gas chromatographic analysis. Derivatives of other amine compounds were prepared to evaluate possible interferences.