M. Rathke
Apr 28, 2003
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Journal
Organic Syntheses
Abstract
β-Hydroxy Esters from Ethyl Acetate and Aldehydes or Ketones: Ethyl 1-hydroxycyclohexylacetate reactant: 42.2 g. (0.263 mole) of hexamethyldisilazane byproduct: hexamethyldisiloxane product: Ethyl 1-hydroxycyclohexylacetate Keywords: addition, to CO; esterification, of substituted monobasic acids; ethyl lithioacetate; lithium bis(trimethylsilyl)amide; tetrahydrofuran; butane; bubbler, mercury