Y. Tamaru, Hirofumi Ochiai, Tatsuya Nakamura
Apr 28, 2003
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Journal
Organic Syntheses
Abstract
Ethyl 5-oxo-6-methyl-6-heptenoate from methacryloyl chloride and ethyl 4-iodobutyrate reactant: 13.8 g (57 mmol) of ethyl 4-iodobutyrate product: ethyl 5-oxo-6-methyl-6-heptenoate Keywords: acylation; metalation reactions, zinc; metal-catalyzed reactions, palladium; replacement reactions, halogen by halogen; benzene; (3-carboethoxypropyl)zinc iodide; N,N-dimethylacetamide; methacryloyl chloride; zinc-copper couple, preparation