A. Konno, Moriyasu Shimojo, T. Fuchigami
Feb 2, 1998
Citations
0
Influential Citations
13
Citations
Journal
Journal of Fluorine Chemistry
Abstract
Abstract Anodic fluorinations of ethyl isonicotinate ( 1 ) and related compounds have been attempted. Desired fluorinated product, 2-fluoroisonicotinate ( 2 ) was obtained in reasonable yield by direct anodic monofluorination of ethyl isonicotinate 1 . The yield of 2 and the conversion of the electrochemical reaction could be improved by applying relatively lower anodic potential and by increasing the concentration of supporting electrolyte Et 3 N · 3HF.