C. Gehrke, D. Lakings
1971
Citations
0
Influential Citations
36
Citations
Journal
Journal of Chromatography A
Abstract
Abstract The major purpose of this investigation was to develop a quantitative method for the gas-liquid chromatographic analysis of the purine and pyrimidine bases at a macro (100 μg), semimicro (10 μg), and micro 500 ng) level. Included was an evaluation of bis (trimethylsilyl) trifluoroacetamide as the silylating reagent, solvents, and the determination of the optimum silylating and instrumental conditions at each level.