L. Jun
2012
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Journal
Science & Technology Vision
Abstract
1-bromobutane was synthesized from n-butyl alcohol, (red) phosphorus and liquid bromine using sulphuric acid as catalyst. Various affecting factors were investigated. The results showed that the optimum conditions were n-butyl alcohol 0.2mo1, (red) phosphorus 0.053mol, distilled water 0.06 mol, liquid bromine 0.08mol and sulphuric acid 0.046 mol, refluxed for 2h, the separated yield was high up to 83%.