M. Jing, Che Bao-quan, Lu Xue-le
2010
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Journal
Journal of Tianjin Institute of Technology
Abstract
Fenticonazole nitrate was synthesized by a new route and the reaction conditions was improved.Compared with the method reported,the present route has several advantages of convenient operation,mild reaction conditions and stable yield.This method is fit for industrial process.The results show that the optimum condititions were: tetrahydrofuran was used as the solvent,the reaction temperature was 25 ℃ and the reaction time was 10 h.The overall yield was result 21.3%.Its structure was characterized by elemental analysis,IR,1H-NMR and MS.