Zhigang Jian, T. Ray, Amy Wu
Oct 15, 2006
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Journal
Journal of Labelled Compounds and Radiopharmaceuticals
Abstract
Summary [ 13 C6]6-Hydroxychlorzoxazone, a major P450 metabolite of chlorzoxazone, was synthesized from [ 13 C6]benzene in an overall 18% yield. An improved procedure for converting 4-chloro-6-nitrosoresorcinol to 6-hydroxychlorzoxazone was developed, with a yield more than double that previously reported in the literature. Copyright # 2006 John Wiley & Sons, Ltd.