J. Shockcor, R. Wurm, I. S. Silver
Jul 11, 1994
Citations
0
Influential Citations
9
Citations
Journal
Tetrahedron Letters
Abstract
The structure of the epoxide of 1-ethyl-phenoxathiin 10,10-dioxide, a potential monoamine oxidase-A inhibitor, was elucidated using a combination of 500 MHz homo- and heteronuclear NMR techniques. The proton reference spectrum and a COSY spectrum were obtained on a 30 μg sample (0.07 μMoles) of the metabolite in 35 μl of d6-DMSO using a Varian heteronuclear Nano-probe™. An inverse-detected (HMQC) heteronuclear shift correlation spectrum was obtained on the 30 μg sample of the metabolite in 120 μl of d6-DMSO using a Nalorac Z•SPEC™ 3 mm micro inverse probe.