S. Mori, I. Sakai, T. Aoyama
Sep 25, 1982
Citations
0
Influential Citations
27
Citations
Journal
Chemical & Pharmaceutical Bulletin
Abstract
The stable and safe compound trimethylsilyldiazomethane (TMSCHN2), which is useful for organic synthesis, was prepared in high yield by diazo-transfer reaction of trimethylsilylmethylmagnesium chloride with diphenyl phosphorazidate [DPPA, (C6H5O)2-P (O) N3].